TA Instruments

AR1704-0001f

04/09/2012 16:11:28

Sample name	ASW 10 mm from base, 60 mm to top, disk 17 PMMA+FA fouled AND CLEANED
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1704
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 16:11:28

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-14.59	7.375	-1.979	1.0080	22.4	205.0	5.3326	10000	0.05032	3.769	6.6658	666.58	3.384E-3	0.0	1.0	61.008	-44.772	5.900
0.6962	12.24	0.05687	2.0240	22.4	195.1	13.1570	10000	0.04788	1.302	16.446	1644.6	3.384E-3	0.0	1.0	62.024	2.1360	9.794
1.508	19.33	0.07805	3.0200	22.4	196.7	26.9915	10000	0.04829	0.5267	33.739	3373.9	3.384E-3	0.1	1.1	63.020	4.6280	15.46
2.071	23.00	0.09005	4.0200	22.4	203.4	40.7482	10000	0.04991	0.3844	50.935	5093.5	3.384E-3	0.1	1.1	64.020	6.3546	18.40
3.333	30.81	0.1082	5.0080	22.4	197.6	67.4561	10000	0.04849	0.2081	84.320	8432.0	3.384E-3	0.1	1.1	65.008	10.227	24.65
5.099	39.46	0.1292	6.0080	22.4	205.0	106.5730	10000	0.05032	0.1317	133.22	13322	3.384E-3	0.1	1.1	66.008	15.643	31.57
5.914	42.51	0.1391	7.0040	22.4	202.5	126.2140	10000	0.04971	0.1121	157.77	15777	3.384E-3	0.1	1.1	67.004	18.144	34.01
7.448	49.11	0.1516	8.0200	22.4	196.7	165.1290	10000	0.04829	0.08157	206.41	20641	3.384E-3	0.1	1.1	68.020	22.849	39.29
9.992	57.53	0.1737	9.0200	22.4	189.3	223.0640	10000	0.04646	0.05721	278.83	27883	3.384E-3	0.2	1.2	69.020	30.656	46.02
11.89	63.68	0.1867	10.020	22.4	190.1	274.5960	10000	0.04666	0.04689	343.25	34325	3.384E-3	0.2	1.2	70.020	36.465	50.94
13.76	69.64	0.1976	11.016	22.4	192.6	326.1610	10000	0.04727	0.03972	407.70	40770	3.384E-3	0.2	1.2	71.016	42.221	55.71
15.72	75.10	0.2093	12.000	22.4	190.1	377.0310	10000	0.04666	0.03371	471.29	47129	3.384E-3	0.2	1.2	72.000	48.235	60.08
17.52	80.50	0.2177	13.020	22.4	182.7	434.5620	10000	0.04484	0.02819	543.20	54320	3.384E-3	0.2	1.2	73.020	53.759	64.40
19.75	86.42	0.2285	14.008	22.4	180.2	498.4790	10000	0.04423	0.02413	623.10	62310	3.384E-3	0.2	1.2	74.008	60.578	69.13
22.76	94.59	0.2406	15.004	22.4	178.6	594.0530	10000	0.04382	0.01996	742.57	74257	3.384E-3	0.3	1.3	75.004	69.830	75.67
24.84	99.90	0.2486	16.012	22.4	175.3	664.1290	10000	0.04301	0.01756	830.16	83016	3.384E-3	0.3	1.3	76.012	76.205	79.92
27.22	105.7	0.2576	17.020	22.4	155.4	740.4850	10000	0.03814	0.01392	925.61	92561	3.384E-3	0.3	1.3	77.020	83.506	84.52
30.35	113.7	0.2668	18.008	22.4	168.6	855.5740	10000	0.04139	0.01304	1069.5	1.0695E5	3.384E-3	0.3	1.3	78.008	93.099	90.98
32.46	118.8	0.2733	19.024	22.4	165.3	931.1080	10000	0.04058	0.01172	1163.9	1.1639E5	3.383E-3	0.3	1.3	79.024	99.590	95.03
35.36	124.2	0.2846	20.024	22.4	160.4	1020.0400	10000	0.03936	0.01039	1275.1	1.2751E5	3.383E-3	0.3	1.3	80.024	108.49	99.40
39.05	132.3	0.2952	21.020	22.4	157.1	1153.3300	10000	0.03855	8.976E-3	1441.7	1.4417E5	3.384E-3	0.4	1.4	81.020	119.80	105.8
41.66	137.4	0.3033	22.024	22.4	151.3	1242.0200	10000	0.03713	8.017E-3	1552.5	1.5525E5	3.384E-3	0.4	1.4	82.024	127.81	109.9
44.47	142.8	0.3115	23.020	22.4	152.1	1344.4301	10000	0.03733	7.460E-3	1680.5	1.6805E5	3.384E-3	0.4	1.4	83.020	136.44	114.2
47.93	150.8	0.3179	24.024	22.4	155.4	1498.1400	10000	0.03814	6.833E-3	1872.7	1.8727E5	3.384E-3	0.4	1.4	84.024	147.06	120.6
50.68	155.9	0.3251	25.016	22.4	145.5	1597.3500	10000	0.03571	5.985E-3	1996.7	1.9967E5	3.384E-3	0.4	1.4	85.016	155.50	124.7
53.65	161.3	0.3326	26.020	22.4	156.2	1710.8800	10000	0.03835	6.004E-3	2138.6	2.1386E5	3.384E-3	0.4	1.4	86.020	164.59	129.1
57.65	169.3	0.3405	27.004	22.4	137.2	1882.9200	10000	0.03368	4.787E-3	2353.7	2.3537E5	3.384E-3	0.5	1.5	87.004	176.88	135.4
60.56	174.4	0.3472	28.004	22.4	146.3	1995.5900	10000	0.03591	4.809E-3	2494.5	2.4945E5	3.384E-3	0.5	1.5	88.004	185.78	139.5
63.09	179.6	0.3514	29.020	22.4	136.4	2115.8601	10000	0.03348	4.231E-3	2644.8	2.6448E5	3.384E-3	0.5	1.5	89.020	193.57	143.6
69.01	187.5	0.3680	30.020	22.4	127.3	2306.2500	10000	0.03125	3.619E-3	2882.8	2.8828E5	3.384E-3	0.5	1.5	90.020	211.71	150.0
72.38	192.7	0.3757	31.000	22.4	112.4	2432.1699	10000	0.02759	3.028E-3	3040.2	3.0402E5	3.384E-3	0.5	1.5	91.000	222.07	154.2
75.66	200.5	0.3773	32.020	22.4	121.5	2635.7500	10000	0.02983	3.022E-3	3294.7	3.2947E5	3.383E-3	0.5	1.5	92.020	232.11	160.4
78.79	205.8	0.3828	33.008	22.4	120.7	2773.6299	10000	0.02962	2.849E-3	3467.0	3.4670E5	3.383E-3	0.6	1.6	93.008	241.73	164.7
82.39	211.0	0.3905	34.004	22.4	112.4	2913.2400	10000	0.02759	2.526E-3	3641.6	3.6416E5	3.384E-3	0.6	1.6	94.004	252.78	168.8
86.55	218.6	0.3959	35.024	22.4	117.4	3127.4099	10000	0.02881	2.456E-3	3909.3	3.9093E5	3.383E-3	0.6	1.6	95.024	265.52	174.9
91.15	223.9	0.4071	36.024	22.4	91.76	3279.8101	10000	0.02252	1.830E-3	4099.8	4.0998E5	3.384E-3	0.6	1.6	96.024	279.63	179.1
93.60	229.1	0.4086	37.008	22.4	97.54	3507.6201	10000	0.02394	1.859E-3	4384.5	4.3845E5	3.384E-3	0.6	1.6	97.008	287.17	183.3
99.38	236.6	0.4200	38.016	22.4	95.07	3659.4099	10000	0.02333	1.698E-3	4574.3	4.5743E5	3.384E-3	0.6	1.6	98.016	304.88	189.3
103.3	241.8	0.4270	39.020	22.4	95.07	3823.7200	10000	0.02333	1.626E-3	4779.7	4.7797E5	3.384E-3	0.7	1.7	99.020	316.82	193.5
108.4	249.6	0.4342	40.008	22.4	95.89	4068.3899	10000	0.02354	1.539E-3	5085.5	5.0855E5	3.384E-3	0.7	1.7	100.008	332.48	199.7
111.1	254.6	0.4365	41.024	22.4	101.7	4232.5000	10000	0.02496	1.568E-3	5290.6	5.2906E5	3.383E-3	0.7	1.7	101.024	340.95	203.7
118.3	262.5	0.4508	42.020	22.4	94.24	4498.8198	10000	0.02313	1.368E-3	5623.5	5.6235E5	3.384E-3	0.7	1.7	102.020	362.98	210.0
121.0	267.6	0.4521	43.020	22.4	58.69	4676.6299	10000	0.01441	8.196E-4	5845.8	5.8458E5	3.383E-3	0.7	1.7	103.020	371.17	214.1
124.2	272.7	0.4557	44.020	22.4	71.92	4850.9902	10000	0.01765	9.673E-4	6063.7	6.0637E5	3.383E-3	0.7	1.7	104.020	381.18	218.1
128.8	280.3	0.4595	45.024	22.4	70.27	5128.7202	10000	0.01725	8.941E-4	6410.9	6.4109E5	3.383E-3	0.8	1.8	105.024	395.24	224.3
133.9	285.5	0.4690	46.024	22.4	58.69	5317.9302	10000	0.01441	7.199E-4	6647.4	6.6474E5	3.384E-3	0.8	1.8	106.024	410.83	228.4
140.4	293.1	0.4791	47.020	22.4	42.99	5601.8999	10000	0.01055	5.003E-4	7002.4	7.0024E5	3.384E-3	0.8	1.8	107.020	430.79	234.5
142.5	298.1	0.4779	48.004	22.4	58.69	5797.4600	10000	0.01441	6.603E-4	7246.8	7.2468E5	3.384E-3	0.8	1.8	108.004	437.14	238.5
150.3	303.3	0.4955	49.008	22.4	35.55	5999.4199	10000	8.724E-3	3.864E-4	7499.3	7.4993E5	3.384E-3	0.8	1.8	109.008	461.06	242.7
154.0	311.0	0.4952	50.020	22.4	42.16	6302.1802	10000	0.01035	4.360E-4	7877.7	7.8777E5	3.384E-3	0.8	1.8	110.020	472.37	248.8
158.5	316.0	0.5016	51.000	22.4	33.07	6511.2900	10000	8.116E-3	3.311E-4	8139.1	8.1391E5	3.383E-3	0.9	1.9	111.000	486.34	252.8
163.2	323.8	0.5041	52.020	22.4	48.77	6831.8799	10000	0.01197	4.652E-4	8539.9	8.5399E5	3.383E-3	0.9	1.9	112.020	500.71	259.0
168.1	328.9	0.5111	53.004	22.4	1.653	7046.3599	10000	4.058E-4	1.529E-5	8808.0	8.8080E5	3.384E-3	0.9	1.9	113.004	515.64	263.1
175.7	336.4	0.5222	54.020	22.4	30.59	7374.1602	10000	7.507E-3	2.703E-4	9217.7	9.2177E5	3.384E-3	0.9	1.9	114.020	538.94	269.1
179.0	341.6	0.5240	55.016	22.4	10.75	7601.3101	10000	2.638E-3	9.209E-5	9501.6	9.5016E5	3.383E-3	0.9	1.9	115.016	549.14	273.3
184.2	346.7	0.5314	56.004	22.4	-9.093	7828.1899	10000	-2.232E-3	-7.565E-5	9785.2	9.7852E5	3.383E-3	0.9	1.9	116.004	565.19	277.4
191.1	354.2	0.5394	57.004	22.4	3.307	8170.2598	10000	8.116E-4	2.635E-5	10213	1.0213E6	3.383E-3	1.0	2.0	117.004	586.15	283.4
193.4	359.3	0.5382	58.020	22.4	23.97	8408.5000	10000	5.884E-3	1.857E-4	10511	1.0511E6	3.384E-3	1.0	2.0	118.020	593.33	287.5
202.6	367.0	0.5520	59.020	22.4	19.84	8767.5000	10000	4.869E-3	1.473E-4	10959	1.0959E6	3.384E-3	1.0	2.0	119.020	621.51	293.6
206.7	372.0	0.5556	60.004	22.4	14.05	9013.6602	10000	3.449E-3	1.015E-4	11267	1.1267E6	3.384E-3	1.0	2.0	120.004	634.09	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

211.7	375.0	0.5645	1.0040	22.4	-39.68	303.1530	10000	-9.739E-3	-2.821E-4	378.94	37894	3.384E-3	0.0	2.0	122.004	649.42	300.0
210.0	375.0	0.5600	2.0000	22.4	-38.03	554.6490	10000	-9.333E-3	-2.704E-4	693.31	69331	3.384E-3	0.0	2.1	123.000	644.22	300.0
209.6	375.0	0.5588	3.0040	22.4	-8.267	805.9390	10000	-2.029E-3	-5.878E-5	1007.4	1.0074E5	3.384E-3	0.1	2.1	124.004	642.92	300.0
209.4	375.0	0.5584	4.0040	22.4	-4.960	1182.9301	10000	-1.217E-3	-3.527E-5	1478.7	1.4787E5	3.384E-3	0.1	2.1	125.004	642.44	300.0
213.1	375.0	0.5682	5.0000	22.4	-48.77	1435.5601	10000	-0.01197	-3.468E-4	1794.5	1.7945E5	3.383E-3	0.1	2.1	126.000	653.67	300.0
210.7	375.0	0.5618	6.0040	22.4	-5.787	1811.4399	10000	-1.420E-3	-4.115E-5	2264.3	2.2643E5	3.384E-3	0.1	2.1	127.004	646.31	300.0
210.0	375.0	0.5601	7.0040	22.4	4.960	2064.9199	10000	1.217E-3	3.527E-5	2581.2	2.5812E5	3.384E-3	0.1	2.1	128.004	644.39	300.0
212.4	375.0	0.5665	8.0160	22.4	-27.28	2314.0000	10000	-6.695E-3	-1.940E-4	2892.5	2.8925E5	3.384E-3	0.1	2.2	129.016	651.75	300.0
211.1	375.0	0.5629	9.0000	22.4	-26.45	2690.7400	10000	-6.493E-3	-1.881E-4	3363.4	3.3634E5	3.384E-3	0.2	2.2	130.000	647.55	300.0
210.3	375.0	0.5607	10.004	22.4	-7.440	2942.0701	10000	-1.826E-3	-5.291E-5	3677.6	3.6776E5	3.384E-3	0.2	2.2	131.004	645.06	300.0
213.3	375.0	0.5689	11.004	22.4	-24.80	3319.4099	10000	-6.087E-3	-1.764E-4	4149.3	4.1493E5	3.384E-3	0.2	2.2	132.004	654.48	300.0
212.9	375.0	0.5677	12.000	22.4	-26.45	3570.5200	10000	-6.493E-3	-1.881E-4	4463.2	4.4632E5	3.384E-3	0.2	2.2	133.000	653.18	300.0
212.3	375.0	0.5662	13.020	22.4	-9.920	3828.3201	10000	-2.435E-3	-7.054E-5	4785.4	4.7854E5	3.383E-3	0.2	2.2	134.020	651.44	300.0
211.4	375.0	0.5638	14.004	22.4	-21.49	4198.7900	10000	-5.275E-3	-1.528E-4	5248.5	5.2485E5	3.383E-3	0.2	2.3	135.004	648.69	300.0
211.1	375.0	0.5630	15.016	22.4	-20.67	4450.1401	10000	-5.072E-3	-1.470E-4	5562.7	5.5627E5	3.383E-3	0.3	2.3	136.016	647.75	300.0
210.3	375.0	0.5608	16.024	22.4	-19.01	4832.3301	10000	-4.666E-3	-1.352E-4	6040.4	6.0404E5	3.383E-3	0.3	2.3	137.024	645.22	300.0
209.6	375.0	0.5588	17.016	22.4	-24.80	5078.3198	10000	-6.087E-3	-1.763E-4	6347.9	6.3479E5	3.384E-3	0.3	2.3	138.016	642.95	300.0
212.9	375.0	0.5678	18.016	22.4	-38.85	5329.7300	10000	-9.536E-3	-2.763E-4	6662.2	6.6622E5	3.383E-3	0.3	2.3	139.016	653.21	300.0
209.5	375.0	0.5586	19.000	22.4	-16.53	5706.8198	10000	-4.058E-3	-1.176E-4	7133.5	7.1335E5	3.384E-3	0.3	2.3	140.000	642.65	300.0
210.6	375.0	0.5615	20.004	22.4	-35.55	5958.0098	10000	-8.724E-3	-2.528E-4	7447.5	7.4475E5	3.384E-3	0.3	2.4	141.004	646.01	300.0
210.0	375.0	0.5599	21.016	22.4	-20.67	6209.6401	10000	-5.072E-3	-1.470E-4	7762.1	7.7621E5	3.383E-3	0.4	2.4	142.016	644.21	300.0
208.1	375.0	0.5550	22.004	22.4	-1.45E-11	6586.2900	10000	-3.55E-15	-1.03E-16	8232.9	8.2329E5	3.383E-3	0.4	2.4	143.004	638.49	300.0
208.0	375.0	0.5547	23.016	22.4	-4.960	6838.1001	10000	-1.217E-3	-3.527E-5	8547.6	8.5476E5	3.384E-3	0.4	2.4	144.016	638.17	300.0
210.3	375.0	0.5609	24.004	22.4	-4.133	7214.6099	10000	-1.014E-3	-2.939E-5	9018.3	9.0183E5	3.384E-3	0.4	2.4	145.004	645.32	300.0
209.9	375.0	0.5596	25.000	22.4	-20.67	7466.2300	10000	-5.072E-3	-1.470E-4	9332.8	9.3328E5	3.384E-3	0.4	2.4	146.000	643.82	300.0
209.4	375.0	0.5585	26.016	22.4	-33.07	7717.4399	10000	-8.116E-3	-2.351E-4	9646.8	9.6468E5	3.384E-3	0.4	2.5	147.016	642.50	300.0
208.1	375.0	0.5548	27.000	22.4	2.480	8094.2798	10000	6.087E-4	1.763E-5	10118	1.0118E6	3.384E-3	0.5	2.5	148.000	638.32	300.0
209.0	375.0	0.5573	28.000	22.4	-17.36	8345.6699	10000	-4.261E-3	-1.234E-4	10432	1.0432E6	3.383E-3	0.5	2.5	149.000	641.23	300.0
206.5	375.0	0.5507	29.004	22.4	-21.49	8726.5195	10000	-5.275E-3	-1.528E-4	10908	1.0908E6	3.384E-3	0.5	2.5	150.004	633.57	300.0
212.1	375.0	0.5657	30.016	22.4	-37.20	8974.0801	10000	-9.130E-3	-2.645E-4	11218	1.1218E6	3.384E-3	0.5	2.5	151.016	650.82	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

204.8	370.6	0.5527	1.0040	22.4	1.653	298.0090	10000	4.058E-4	1.204E-5	372.51	37251	3.383E-3	0.0	2.5	152.004	628.46	296.5
200.5	365.6	0.5485	2.0200	22.4	-9.920	535.9960	10000	-2.435E-3	-7.421E-5	670.00	67000	3.383E-3	0.0	2.6	153.020	615.25	292.5
194.1	358.0	0.5423	3.0200	22.4	11.57	892.9590	10000	2.840E-3	9.031E-5	1116.2	1.1162E5	3.384E-3	0.1	2.6	154.020	595.55	286.4
191.3	352.8	0.5423	4.0080	22.4	-19.01	1130.7600	10000	-4.666E-3	-1.528E-4	1413.5	1.4135E5	3.384E-3	0.1	2.6	155.008	586.97	282.2
187.5	347.7	0.5391	5.0040	22.4	19.01	1470.8400	10000	4.666E-3	1.572E-4	1838.6	1.8386E5	3.383E-3	0.1	2.6	156.004	575.14	278.2
180.3	340.1	0.5300	6.0200	22.4	-14.05	1694.4600	10000	-3.449E-3	-1.215E-4	2118.1	2.1181E5	3.384E-3	0.1	2.6	157.020	553.13	272.1
174.7	335.0	0.5214	7.0200	22.4	-3.307	1919.8300	10000	-8.116E-4	-2.947E-5	2399.8	2.3998E5	3.384E-3	0.1	2.6	158.020	535.90	268.0
168.8	327.5	0.5154	8.0360	22.4	32.24	2244.3401	10000	7.913E-3	3.007E-4	2805.4	2.8054E5	3.384E-3	0.1	2.7	159.036	517.82	262.0
163.6	322.4	0.5075	9.0160	22.4	12.40	2451.8501	10000	3.043E-3	1.193E-4	3064.8	3.0648E5	3.384E-3	0.2	2.7	160.016	501.92	257.9
157.9	314.6	0.5019	10.004	22.4	49.60	2771.2700	10000	0.01217	5.010E-4	3464.1	3.4641E5	3.384E-3	0.2	2.7	161.004	484.49	251.7
154.6	309.6	0.4994	11.016	22.4	33.89	2971.5400	10000	8.319E-3	3.536E-4	3714.4	3.7144E5	3.384E-3	0.2	2.7	162.016	474.32	247.7
143.5	302.0	0.4752	12.020	22.4	15.71	3275.9700	10000	3.855E-3	1.722E-4	4095.0	4.0950E5	3.383E-3	0.2	2.7	163.020	440.29	241.6
142.5	296.8	0.4801	13.008	22.4	48.77	3481.5200	10000	0.01197	5.536E-4	4351.9	4.3519E5	3.383E-3	0.2	2.7	164.008	437.18	237.5
139.0	291.6	0.4767	14.004	22.4	44.64	3666.5500	10000	0.01096	5.249E-4	4583.2	4.5832E5	3.383E-3	0.2	2.8	165.004	426.55	233.3
133.0	284.1	0.4681	15.020	22.4	62.00	3947.8101	10000	0.01522	7.684E-4	4934.8	4.9348E5	3.384E-3	0.3	2.8	166.020	407.93	227.2
131.0	278.9	0.4697	16.020	22.4	62.00	4135.5400	10000	0.01522	7.970E-4	5169.4	5.1694E5	3.384E-3	0.3	2.8	167.020	401.88	223.1
125.5	271.3	0.4627	17.020	22.4	62.00	4405.5898	10000	0.01522	8.426E-4	5507.0	5.5070E5	3.384E-3	0.3	2.8	168.020	385.04	217.0
122.1	266.2	0.4586	18.020	22.4	76.88	4580.0498	10000	0.01887	1.085E-3	5725.1	5.7251E5	3.384E-3	0.3	2.8	169.020	374.59	213.0
116.6	261.1	0.4468	19.020	22.4	70.27	4754.8101	10000	0.01725	1.031E-3	5943.5	5.9435E5	3.384E-3	0.3	2.8	170.020	357.85	208.9
111.6	253.3	0.4408	20.004	22.4	92.59	5011.0698	10000	0.02272	1.443E-3	6263.8	6.2638E5	3.384E-3	0.3	2.9	171.004	342.53	202.6
109.0	248.3	0.4390	21.004	22.4	84.32	5173.6099	10000	0.02069	1.368E-3	6467.0	6.4670E5	3.384E-3	0.4	2.9	172.004	334.34	198.6
102.1	240.5	0.4243	22.020	22.4	76.88	5417.5801	10000	0.01887	1.329E-3	6772.0	6.7720E5	3.383E-3	0.4	2.9	173.020	313.12	192.4
98.77	235.2	0.4199	23.020	22.4	83.49	5579.8799	10000	0.02049	1.509E-3	6974.9	6.9749E5	3.383E-3	0.4	2.9	174.020	303.02	188.2
95.78	230.2	0.4162	24.004	22.4	83.49	5807.8301	10000	0.02049	1.576E-3	7259.8	7.2598E5	3.384E-3	0.4	2.9	175.004	293.86	184.1
90.19	222.5	0.4054	25.020	22.4	109.9	5955.0698	10000	0.02698	2.221E-3	7443.8	7.4438E5	3.384E-3	0.4	2.9	176.020	276.69	178.0
86.95	217.2	0.4003	26.004	22.4	95.89	6106.7300	10000	0.02354	2.033E-3	7633.4	7.6334E5	3.384E-3	0.4	3.0	177.004	266.75	173.8
82.47	209.6	0.3935	27.020	22.4	110.8	6311.8101	10000	0.02719	2.521E-3	7889.8	7.8898E5	3.384E-3	0.5	3.0	178.020	253.02	167.7
78.04	204.5	0.3817	28.020	22.4	111.6	6449.5698	10000	0.02739	2.669E-3	8062.0	8.0620E5	3.384E-3	0.5	3.0	179.020	239.43	163.6
74.39	199.2	0.3734	29.020	22.4	122.3	6586.6899	10000	0.03003	3.083E-3	8233.4	8.2334E5	3.384E-3	0.5	3.0	180.020	228.22	159.4
69.74	191.4	0.3644	30.004	22.4	124.0	6780.1499	10000	0.03043	3.385E-3	8475.2	8.4752E5	3.384E-3	0.5	3.0	181.004	213.96	153.1
66.61	186.3	0.3576	31.004	22.4	130.6	6904.2998	10000	0.03206	3.763E-3	8630.4	8.6304E5	3.383E-3	0.5	3.0	182.004	204.36	149.0
62.69	178.4	0.3515	32.008	22.4	120.7	7092.7998	10000	0.02962	3.794E-3	8866.0	8.8660E5	3.384E-3	0.5	3.1	183.008	192.34	142.7
59.71	173.0	0.3451	33.020	22.4	139.7	7210.1001	10000	0.03429	4.668E-3	9012.6	9.0126E5	3.384E-3	0.6	3.1	184.020	183.18	138.4
57.78	167.9	0.3442	34.020	22.4	128.1	7322.3999	10000	0.03145	4.545E-3	9153.0	9.1530E5	3.384E-3	0.6	3.1	185.020	177.28	134.3
52.49	160.0	0.3281	35.000	22.4	135.6	7490.7300	10000	0.03327	5.299E-3	9363.4	9.3634E5	3.384E-3	0.6	3.1	186.000	161.04	128.0
50.02	154.6	0.3236	36.044	22.4	134.7	7596.6401	10000	0.03307	5.639E-3	9495.8	9.4958E5	3.383E-3	0.6	3.1	187.044	153.47	123.7
47.08	149.5	0.3149	37.004	22.4	148.8	7696.7002	10000	0.03652	6.657E-3	9620.9	9.6209E5	3.383E-3	0.6	3.1	188.004	144.45	119.6
44.00	141.6	0.3108	38.008	22.4	148.0	7845.8901	10000	0.03632	7.384E-3	9807.4	9.8074E5	3.383E-3	0.6	3.2	189.008	134.99	113.3
40.74	136.2	0.2992	39.020	22.4	162.9	7940.6201	10000	0.03997	8.780E-3	9925.8	9.9258E5	3.383E-3	0.7	3.2	190.020	125.00	109.0
38.46	131.1	0.2933	40.020	22.4	174.4	8026.9399	10000	0.04281	0.01014	10034	1.0034E6	3.384E-3	0.7	3.2	191.020	118.00	104.9
34.81	123.2	0.2825	41.020	22.4	177.7	8157.5898	10000	0.04362	0.01171	10197	1.0197E6	3.383E-3	0.7	3.2	192.020	106.78	98.55
32.06	117.6	0.2726	42.016	22.4	154.6	8244.1504	10000	0.03794	0.01118	10305	1.0305E6	3.384E-3	0.7	3.2	193.016	98.365	94.08
29.10	112.4	0.2590	43.020	22.4	147.1	8323.2100	10000	0.03611	0.01165	10404	1.0404E6	3.383E-3	0.7	3.2	194.020	89.285	89.90
26.22	104.4	0.2512	44.020	22.4	174.4	8430.7998	10000	0.04281	0.01601	10539	1.0539E6	3.384E-3	0.7	3.3	195.020	80.440	83.50
24.10	98.71	0.2442	45.020	22.4	159.5	8505.0000	10000	0.03916	0.01637	10631	1.0631E6	3.384E-3	0.8	3.3	196.020	73.950	78.97
21.88	93.47	0.2341	46.004	22.4	171.1	8567.3799	10000	0.04200	0.01959	10709	1.0709E6	3.384E-3	0.8	3.3	197.004	67.121	74.78
20.06	85.43	0.2349	47.016	22.4	191.0	8660.2695	10000	0.04687	0.02617	10825	1.0825E6	3.384E-3	0.8	3.3	198.016	61.557	68.34
16.80	79.63	0.2110	48.020	22.4	177.7	8721.7197	10000	0.04362	0.02803	10902	1.0902E6	3.384E-3	0.8	3.3	199.020	51.553	63.70
15.23	74.35	0.2048	49.020	22.4	185.2	8771.1602	10000	0.04545	0.03350	10964	1.0964E6	3.384E-3	0.8	3.3	200.020	46.726	59.48
13.54	69.02	0.1961	50.004	22.4	169.5	8820.7500	10000	0.04159	0.03558	11026	1.1026E6	3.384E-3	0.8	3.4	201.004	41.532	55.21
11.53	63.25	0.1822	51.020	22.4	190.1	8870.2100	10000	0.04666	0.04752	11088	1.1088E6	3.383E-3	0.9	3.4	202.020	35.359	50.60
9.279	54.80	0.1693	52.020	22.4	186.8	8931.1504	10000	0.04585	0.06222	11164	1.1164E6	3.383E-3	0.9	3.4	203.020	28.469	43.84
7.693	49.33	0.1560	53.220	22.4	194.3	8967.8398	10000	0.04768	0.07984	11210	1.1210E6	3.384E-3	0.9	3.4	204.220	23.603	39.46
6.174	43.21	0.1429	54.004	22.4	191.0	9004.2998	10000	0.04687	0.1023	11255	1.1255E6	3.384E-3	0.9	3.4	205.004	18.941	34.57
4.668	36.79	0.1269	55.004	22.4	191.8	9034.5195	10000	0.04707	0.1417	11293	1.1293E6	3.384E-3	0.9	3.4	206.004	14.322	29.43
3.507	31.27	0.1121	56.020	22.4	195.1	9058.7998	10000	0.04788	0.1995	11324	1.1324E6	3.383E-3	0.9	3.5	207.020	10.758	25.02
2.417	24.66	0.09802	57.004	22.4	183.5	9082.2803	10000	0.04504	0.3017	11353	1.1353E6	3.383E-3	1.0	3.5	208.004	7.4165	19.73
1.808	20.69	0.08739	58.020	22.4	199.2	9093.8096	10000	0.04890	0.4655	11367	1.1367E6	3.384E-3	1.0	3.5	209.020	5.5463	16.55
0.9877	14.33	0.06892	59.020	22.4	200.0	9105.3799	10000	0.04910	0.9741	11382	1.1382E6	3.383E-3	1.0	3.5	210.020	3.0301	11.46
0.3439	7.551	0.04554	60.004	22.4	191.8	9113.4004	10000	0.04707	3.364	11392	1.1392E6	3.384E-3	1.0	3.5	211.004	1.0549	6.040

